Graphics

Graphics

Pattern List

Ref.Code     Chem. Formula         Score    Scale Fac.  Mineral Name          
01-070-3755  Si O2                      68       0.901  Quartz                
04-006-6835  Fe S2                      55       0.113  Pyrite, syn           
04-011-6849  K Al2 Si4 O10 ( O ..       32       0.215  Muscovite-2M1         
01-085-2163  ( Mg5.036 Fe4.964 ..       16       0.056  Chamosite-1MIIb       
00-003-0596  Ca C O3                     4       0.230  Calcite               
00-009-0466  Na Al Si3 O8               15       0.034  Albite, ordered       

Peak List

Pos.[°2Th.]  d-spacing [Å]  Rel. Int. [%]  Matched by
     6.2335       14.17937           1.58  01-085-2163       
     8.8571        9.98423           8.29  04-011-6849       
    12.5155        7.07272           5.90  01-085-2163       
    17.7290        5.00289           2.08  04-011-6849       
    18.7878        4.72327           0.72  01-085-2163       
    19.8377        4.47560           4.93  04-011-6849       
    20.8570        4.25913          19.10  01-070-3755;04..  
    21.5473        4.12421           0.30  04-011-6849       
    22.0726        4.02723           0.72  00-009-0466       
    22.9100        3.88190           0.89  04-011-6849;01..  
    23.7651        3.74411           0.97  04-011-6849       
    24.2881        3.66467           0.85  01-085-2163;00..  
    25.1826        3.53649           2.93  01-085-2163       
    26.6303        3.34743         100.00  01-070-3755;04..  
    27.9346        3.19403           2.69  04-011-6849;00..  
    28.5115        3.13070           4.04  04-006-6835;04..  
    29.4713        3.03090           0.81  00-003-0596       
    29.8123        2.99699           1.06  04-011-6849       
    31.2293        2.86417           1.20  04-011-6849;00..  
    33.0280        2.71218          11.94  04-006-6835       
    34.5170        2.59852           2.50  04-011-6849;01..  
    35.0146        2.56272           4.88  04-011-6849;01..  
    36.5358        2.45944           6.99  01-070-3755;04..  
    37.0683        2.42533           7.80  04-006-6835;04..  
    37.6699        2.38796           1.65  04-011-6849;01..  
    38.8678        2.31708           0.73  04-011-6849;01..  
    39.4542        2.28399           5.87  01-070-3755;01..  
    40.2906        2.23848           2.50  01-070-3755;04..  
    40.7461        2.21450           5.50  04-006-6835;04..  
    42.4281        2.13052           5.45  01-070-3755;04..  
    45.3679        1.99907           1.81  04-011-6849;01..  
    45.7658        1.98261           2.95  01-070-3755;04..  
    47.5629        1.91181           4.57  04-006-6835       
    50.1130        1.82034           9.47  01-070-3755;01..  
    51.9820        1.75921           0.57  04-011-6849;01..  
    54.8536        1.67371           2.68  01-070-3755;04..  
    55.2911        1.66150           1.56  01-070-3755;04..  
    56.2442        1.63559           8.74  04-006-6835;04..  
    59.0447        1.56452           1.14  04-006-6835;04..  
    59.9448        1.54316           6.10  01-070-3755;04..  
    61.6703        1.50406           3.21  04-006-6835;04..  
    64.2761        1.44924           2.64  04-006-6835;01..  
    65.8700        1.41798           0.41  01-070-3755;04..  
    67.7233        1.38362           3.34  01-070-3755;01..  
    68.3090        1.37318           4.64  01-070-3755;04..  

Anchor Scan Parameters

Dataset Name:	MT 25
File name:	C:\XRD Data\MT 25.xrdml
Comment:	Configuration=Spinner Srage - Transmission, Owner=User-1, Creation date=11/5/2013 2:01:36 PM
	Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
	Sample stage=Reflection-Transmission Spinner PW3064/60; Minimum step size Phi:0.1
	Diffractometer system=XPERT-PRO
	Measurement program=C:\Users\SEMCAL_XRD\Documents\Marcellus MSEEL\MT 25.xrdmp, Identifier={1DDD3C5C-7085-472B-A66B-5B82501E3549}
	Batch program=C:\PANalytical\Data Collector\Programs\Xcelerator batch.xrdmp, Identifier={2DE27062-C861-455A-B083-8003C05BDEB5}
	MT 25
Measurement Date / Time:	5/24/2016 4:37:52 PM
Operator:	SEMCAL_XRD
Raw Data Origin:	XRD measurement (*.XRDML)
Scan Axis:	Gonio
Start Position [°2Th.]:	5.0084
End Position [°2Th.]:	69.9824
Step Size [°2Th.]:	0.0170
Scan Step Time [s]:	20.3200
Scan Type:	Continuous
PSD Mode:	Scanning
PSD Length [°2Th.]:	2.12
Offset [°2Th.]:	0.0000
Divergence Slit Type:	Fixed
Divergence Slit Size [°]:	0.2177
Specimen Length [mm]:	10.00
Measurement Temperature [°C]:	25.00
Anode Material:	Cu
K-Alpha1 [Å]:	1.54060
K-Alpha2 [Å]:	1.54443
K-Beta [Å]:	1.39225
K-A2 / K-A1 Ratio:	0.50000
Generator Settings:	40 mA, 45 kV
Diffractometer Type:	0000000011117966
Diffractometer Number:	0
Goniometer Radius [mm]:	240.00
Dist. Focus-Diverg. Slit [mm]:	100.00
Incident Beam Monochromator:	No
Spinning:	Yes

Document History

Insert Measurement:
- File name = "MT 25.xrdml"
- Modification time = "9/17/2016 9:28:39 AM"
- Modification editor = "SEMCAL_XRD"

Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
- Modification time = "9/17/2016 9:28:39 AM"
- Modification editor = "SEMCAL_XRD"

Interpolate Step Size:
- Derived = "Yes"
- Step Size = "0.01"
- Modification time = "9/17/2016 9:28:39 AM"
- Modification editor = "PANalytical"

Determine Background:
- Add to net scan = "Nothing"
- User defined intensity = "-5"
- Correction method = "Automatic"
- Bending factor = "2"
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Use smoothed input data = "Yes"
- Granularity = "20"
- Modification time = "8/2/2016 1:27:12 PM"
- Modification editor = "SEMCAL_XRD"

Search Peaks:
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Method = "Minimum 2nd derivative"
- Modification time = "8/18/2016 10:13:32 AM"
- Modification editor = "SEMCAL_XRD"

Search & Match:
- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "9/17/2016 9:29:32 AM"
- Modification editor = "SEMCAL_XRD"

Delete Peak(s):
- Start position = "5.2103"
- End position = "5.2103"
- Modification time = "9/17/2016 9:31:44 AM"
- Modification editor = "SEMCAL_XRD"